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大学・研究所にある論文を検索できる 「Air-stable and reusable nickel phosphide nanoparticle catalyst for the highly selective hydrogenation of d-glucose to d-sorbitol」の論文概要。リケラボ論文検索は、全国の大学リポジトリにある学位論文・教授論文を一括検索できる論文検索サービスです。
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Air-stable and reusable nickel phosphide nanoparticle catalyst for the highly selective hydrogenation of d-glucose to d-sorbitol

Yamaguchi, Sho 大阪大学

2021.03.07

概要

The hydrogenation of carbohydrates to polyols is an industrially important process, but it requires air-unstable, non-noble metal catalysts with low activity and harsh reaction conditions. Herein, we report a hydrotalcite (HT)-supported nickel phosphide nanoparticle (nano-Ni₂P/HT) that exhibits both air stability and high activity for the selective hydrogenation of d-glucose to d-sorbitol in water. The nano-Ni₂P/HT catalyst provides d-sorbitol in excellent yield with >99% selectivity under mild reaction conditions, and is the first non-noble metal catalyst that can operate under just 1 bar of H₂ or at ambient temperature. This high-performance nano-Ni₂P/HT catalyst is significantly different from conventional Ni(0) and NiO nanoparticles and Raney catalysts, which result in almost no production of d-sorbitol, demonstrating the unique catalysis of nano-Ni₂P/HT. Furthermore, nano-Ni₂P/HT shows the highest activity among those reported for non-noble metal catalysts. The nano-Ni₂P/HT catalyst can also be reused without sacrificing its high activity and selectivity. Additionally, the successful transformation of a concentrated d-glucose solution (50 wt%) to d-sorbitol has been achieved. This is the first example of an air-stable, highly active, and reusable non-noble metal catalyst that can replace conventional catalysts used for d-sorbitol production, thus providing a cheap, green, and sustainable route for this process.

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