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Acknowledgements
The diffraction experiments and their preparation works were conducted with the approval
of the Japan Synchrotron Radiation Research Institute. SACLA research proposals:
2019B8032 (complementary use with J-PARC/MLF), 2019A8036 (complementary use with
J-PARC/MLF), 2018A8036, 2018B8039, 2018A8033, 2017B8051, 2017B8080, 2016B8083,
2016B8084, and 2016A8065. SPring-8 research proposal: 2016A1128. This work was supported in part by KAKENHI (grant nos. 20K20947, 20H01965, 17H01172 and 16H02246)
from the Japan Society for the Promotion of Science (JSPS), and X-ray Free Electron Laser
Priority Strategy Programme (contract 12005014 at Osaka University and 12005064 at
Okayama University) and Quantum Leap Flagship Programme (JPMXS0118067246) from
the Ministry of Education, Culture, Sports, Science, and Technology.
Author contributions
T.O., N.T. and N.O. designed the research. T.O., Y.S., N.T., T.M., B.A., N.J.H., Y.I., K.K.,
R.K., T.A.P., N.P., K.M., T.S., T.S., K.S., K.A.T., Y.T., T.T., Y.U., T.Y., M.Y. and N.O.
participated in preparing or conducting the experiments. T.O. analysed the diffraction
data using the software developed by Y.S. T.O., Y.S., N.T., T.M., B.A., N.J.H., Y.I., K.K.,
R.K., T.A.P., N.P., K.M., T.S., T.S., K.S., K.A.T., Y.T., T.T., Y.U., T.Y., M.Y. and N.O.
participated in discussing results. T.O., Y.S. and N.T. wrote the paper.
Competing interests
The authors declare no competing interests.
Additional information
Supplementary information The online version contains supplementary material
available at https://doi.org/10.1038/s41467-021-24633-4.
Correspondence and requests for materials should be addressed to T.O.
Peer review information Nature Communications thanks the anonymous reviewers for
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